Crystallography Open Database

Information card for entry 4309255

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Coordinates	4309255.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H33 N2 Sb
Calculated formula	C24 H33 N2 Sb
Title of publication	Synthetic and Structural Studies of Cyclodistib(V)azanes
Authors of publication	May C. Copsey; Sabrina B. Gallon; Sara K. Grocott; John C. Jeffery; Christopher A. Russell; John M. Slattery
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Pages of publication	5495 - 5500
a	16.7385 ± 0.0006 Å
b	13.1417 ± 0.0004 Å
c	21.354 ± 0.0007 Å
α	90°
β	112.542 ± 0.002°
γ	90°
Cell volume	4338.4 ± 0.3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.029
Residual factor for significantly intense reflections	0.0267
Weighted residual factors for significantly intense reflections	0.0706
Weighted residual factors for all reflections included in the refinement	0.0719
Goodness-of-fit parameter for all reflections included in the refinement	1.094
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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