Information card for entry 4309333

Structure parameters

• Formula: Co5 H68 Na10 O34 S20 Sn5
• Calculated formula: Co4.98 Na10 O34 S20 Sn5.02
• Title of publication: Unusual Syntheses, Structures, and Electronic Properties of Compounds Containing Ternary, T3-Type Supertetrahedral M/Sn/S Anions [M5Sn(μ3-S)4(SnS4)4]10- (M = Zn, Co)
• Authors of publication: Christian Zimmermann; Christopher E. Anson; Florian Weigend; Rodolphe Clérac; Stefanie Dehnen
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Pages of publication: 5686 - 5695
• a: 14.712 ± 0.002 Å
• b: 14.737 ± 0.002 Å
• c: 17.142 ± 0.002 Å
• α: 97.298 ± 0.002°
• β: 99.264 ± 0.002°
• γ: 103.868 ± 0.003°
• Cell volume: 3507.6 ± 0.8 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.116
• Residual factor for significantly intense reflections: 0.0625
• Weighted residual factors for significantly intense reflections: 0.1533
• Weighted residual factors for all reflections included in the refinement: 0.1819
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No