Information card for entry 4309342

Structure parameters

• Formula: C54 H54 N8 Os2 Si2
• Calculated formula: C54 H54 N8 Os2 Si2
• SMILES: [Os]1234([Os](N(c5[n]1cccc5)c1ccccc1)(N(c1[n]2cccc1)c1ccccc1)(N(c1[n]3cccc1)c1ccccc1)([n]1c(N4c2ccccc2)cccc1)C#C[Si](C)(C)C)C#C[Si](C)(C)C
• Title of publication: Diosmium(III) Compounds Supported by 2-Anilinopyridinate and Novel Alkynyl Derivatives
• Authors of publication: Yan-Hui Shi; Wei-Zhong Chen; Kevin D. John; Ryan E. Da Re; Joshua L. Cohn; Guo-Lin Xu; Judith L. Eglin; Alfred P. Sattelberger; Curtis R. Hare; Tong Ren
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Pages of publication: 5719 - 5727
• a: 10.745 ± 0.005 Å
• b: 15.977 ± 0.008 Å
• c: 17.931 ± 0.009 Å
• α: 70.64 ± 0.03°
• β: 87.14 ± 0.06°
• γ: 78.87 ± 0.04°
• Cell volume: 2849 ± 3 ų
• Cell temperature: 300 ± 2 K
• Ambient diffraction temperature: 300 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0889
• Residual factor for significantly intense reflections: 0.047
• Weighted residual factors for significantly intense reflections: 0.1099
• Weighted residual factors for all reflections included in the refinement: 0.1236
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No