Information card for entry 4309385

Structure parameters

• Formula: C33 H53 Al N2 O S2 Si2
• Calculated formula: C33 H53 Al N2 O S2 Si2
• Title of publication: Unusual Anions [LAl(SH)(S)]- and [LAl(S)2]2- Stabilized by Weakly Coordinating Imidazolium Cations. Synthesis of LAl(SSiMe2)2O (L = HC[C(Me)N(Ar)]2, Ar = 2,6-iPr2C6H3)
• Authors of publication: Vojtech Jancik; Herbert W. Roesky
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Pages of publication: 5556 - 5558
• a: 12.749 ± 0.003 Å
• b: 18.857 ± 0.004 Å
• c: 15.726 ± 0.003 Å
• α: 90°
• β: 104.29 ± 0.03°
• γ: 90°
• Cell volume: 3663.7 ± 1.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0296
• Residual factor for significantly intense reflections: 0.0288
• Weighted residual factors for significantly intense reflections: 0.076
• Weighted residual factors for all reflections included in the refinement: 0.0768
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No