Crystallography Open Database

Information card for entry 4309450

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Coordinates	4309450.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C67 H134 B4 K2 O7 Yb
Calculated formula	C67 H124 B4 K2 O7 Yb
Title of publication	Europium(II) and Ytterbium(II) Cyclic Organohydroborates with Agostic Interactions
Authors of publication	Xuenian Chen; Soyoung Lim; Christine E. Plečnik; Shengming Liu; Bin Du; Edward A. Meyers; Sheldon G. Shore
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Pages of publication	6052 - 6061
a	17.6244 ± 0.001 Å
b	19.9528 ± 0.001 Å
c	21.2835 ± 0.001 Å
α	90°
β	95.555 ± 0.01°
γ	90°
Cell volume	7449.3 ± 0.7 Å³
Cell temperature	210 ± 2 K
Ambient diffraction temperature	210 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0357
Residual factor for significantly intense reflections	0.0303
Weighted residual factors for significantly intense reflections	0.0852
Weighted residual factors for all reflections included in the refinement	0.0886
Goodness-of-fit parameter for all reflections included in the refinement	1.072
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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