Crystallography Open Database

Information card for entry 4309476

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Coordinates	4309476.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H56 Cu3 N26
Calculated formula	C24 H56 Cu3 N26
Title of publication	Cation-Dependent Nuclearity of the Copper-Azido Moiety: Synthesis, Structure, and Magnetic Study
Authors of publication	Sandip Saha; Subratanath Koner; Jean-Pierre Tuchagues; Athanassios K. Boudalis; Ken-Ichi Okamoto; Surajit Banerjee; Dasarath Mal
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Pages of publication	6379 - 6385
a	8.811 ± 0.0017 Å
b	37.266 ± 0.003 Å
c	13.796 ± 0.001 Å
α	90°
β	107.05 ± 0.01°
γ	90°
Cell volume	4330.8 ± 1 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0759
Residual factor for significantly intense reflections	0.0457
Weighted residual factors for significantly intense reflections	0.1028
Weighted residual factors for all reflections included in the refinement	0.1197
Goodness-of-fit parameter for all reflections included in the refinement	1.06
Diffraction radiation wavelength	0.7093 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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