Information card for entry 4309755

Structure parameters

• Formula: C60 H54 N3 O19 P3 Re4 U
• Calculated formula: C60 H54 N3 O19 P3 Re4 U
• Title of publication: The Synthesis, Structural, and Spectroscopic Characterization of Uranium(IV) Perrhenate Complexes
• Authors of publication: Gordon H. John; Iain May; Clint A. Sharrad; Andrew D. Sutton; David Collison; Madeleine Helliwell; Mark J. Sarsfield
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Pages of publication: 7606 - 7615
• a: 18.3426 ± 0.0013 Å
• b: 18.5254 ± 0.0013 Å
• c: 19.2253 ± 0.0014 Å
• α: 90°
• β: 95.064 ± 0.001°
• γ: 90°
• Cell volume: 6507.3 ± 0.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.066
• Residual factor for significantly intense reflections: 0.0501
• Weighted residual factors for significantly intense reflections: 0.1231
• Weighted residual factors for all reflections included in the refinement: 0.1356
• Goodness-of-fit parameter for all reflections included in the refinement: 0.971
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No