Crystallography Open Database

Information card for entry 4309891

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Coordinates	4309891.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32.5 H31 N4 O5.5 Pb S2
Calculated formula	C32.5 H31 N4 O5.5 Pb S2
Title of publication	Structural Insights into the Coordination and Extraction of Pb(II) by Disulfonamide Ligands Derived from o-Phenylenediamine
Authors of publication	Robert J. Alvarado; Jay M. Rosenberg; Aileen Andreu; Jeffrey C. Bryan; Wei-Zhong Chen; Tong Ren; Konstantinos Kavallieratos
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Pages of publication	7951 - 7959
a	19.4207 ± 0.0011 Å
b	13.4855 ± 0.0008 Å
c	25.6477 ± 0.0014 Å
α	90°
β	95.159 ± 0.001°
γ	90°
Cell volume	6689.9 ± 0.7 Å³
Cell temperature	300 ± 2 K
Ambient diffraction temperature	300 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0542
Residual factor for significantly intense reflections	0.0356
Weighted residual factors for significantly intense reflections	0.0779
Weighted residual factors for all reflections included in the refinement	0.0813
Goodness-of-fit parameter for all reflections included in the refinement	1.008
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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