Information card for entry 4309894

Structure parameters

• Formula: C66 H78 Cl3 N5 O2 P2 Pd
• Calculated formula: C66 H78 Cl3 N5 O2 P2 Pd
• Title of publication: Palladium and Rhodium Ureaphosphine Complexes: Exploring Structural and Catalytic Consequences of Anion Binding
• Authors of publication: Paul A. Duckmanton; Alexander J. Blake; Jason B. Love
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Pages of publication: 7708 - 7710
• a: 9.4731 ± 0.001 Å
• b: 22.807 ± 0.002 Å
• c: 14.223 ± 0.002 Å
• α: 90°
• β: 90.221 ± 0.002°
• γ: 90°
• Cell volume: 3072.9 ± 0.6 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.0947
• Residual factor for significantly intense reflections: 0.0533
• Weighted residual factors for significantly intense reflections: 0.105
• Weighted residual factors for all reflections included in the refinement: 0.122
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No