Crystallography Open Database

Information card for entry 4310050

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Coordinates	4310050.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C74.5 H105 B2 Cl N2 O13 P4 Ru
Calculated formula	C74.5 H105 B2 Cl N2 O13 P4 Ru
Title of publication	Tautomerization of Methyldiazene to Formaldehyde-Hydrazone in Ruthenium and Osmium Complexes
Authors of publication	Gabriele Albertin; Stefano Antoniutti; Alessia Bacchi; Fabiola De Marchi; Giancarlo Pelizzi
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Pages of publication	8947 - 8954
a	22.239 ± 0.001 Å
b	19.041 ± 0.001 Å
c	19.538 ± 0.001 Å
α	90°
β	90°
γ	90°
Cell volume	8273.4 ± 0.7 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	8
Space group number	29
Hermann-Mauguin space group symbol	P c a 21
Hall space group symbol	P 2c -2ac
Residual factor for all reflections	0.0702
Residual factor for significantly intense reflections	0.0465
Weighted residual factors for significantly intense reflections	0.1137
Weighted residual factors for all reflections included in the refinement	0.1216
Goodness-of-fit parameter for all reflections included in the refinement	0.957
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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