Information card for entry 4310125

Structure parameters

• Formula: C6 H24 La N6 S4 Sb
• Calculated formula: C6 H24 La N6 S4 Sb
• Title of publication: Solvothermal Syntheses of [Ln(en)3(H2O)x(μ3-x-SbS4)] (Ln = La,x= 0; Ln = Nd,x= 1) and [Ln(en)4]SbS4.0.5en (Ln = Eu, Dy, Yb): A Systematic Study on the Formation and Crystal Structures of New Lanthanide Thioantimonates(V)
• Authors of publication: Dingxian Jia; Qianxin Zhao; Yong Zhang; Jie Dai; Jinglin Zuo
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Pages of publication: 8861 - 8867
• a: 8.723 ± 0.0015 Å
• b: 10.2043 ± 0.0019 Å
• c: 20.277 ± 0.004 Å
• α: 90°
• β: 93.818 ± 0.005°
• γ: 90°
• Cell volume: 1800.9 ± 0.6 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0385
• Residual factor for significantly intense reflections: 0.0358
• Weighted residual factors for significantly intense reflections: 0.0577
• Weighted residual factors for all reflections included in the refinement: 0.0583
• Goodness-of-fit parameter for all reflections included in the refinement: 1.324
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No