Information card for entry 4310129

Structure parameters

• Formula: C9 H36 N9 S4 Sb Yb
• Calculated formula: C9 H30 N9 S4 Sb Yb
• Title of publication: Solvothermal Syntheses of [Ln(en)3(H2O)x(μ3-x-SbS4)] (Ln = La,x= 0; Ln = Nd,x= 1) and [Ln(en)4]SbS4.0.5en (Ln = Eu, Dy, Yb): A Systematic Study on the Formation and Crystal Structures of New Lanthanide Thioantimonates(V)
• Authors of publication: Dingxian Jia; Qianxin Zhao; Yong Zhang; Jie Dai; Jinglin Zuo
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Pages of publication: 8861 - 8867
• a: 11.0482 ± 0.0007 Å
• b: 12.8801 ± 0.0008 Å
• c: 16.0753 ± 0.001 Å
• α: 90°
• β: 91.966 ± 0.002°
• γ: 90°
• Cell volume: 2286.2 ± 0.2 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0429
• Residual factor for significantly intense reflections: 0.0397
• Weighted residual factors for significantly intense reflections: 0.0926
• Weighted residual factors for all reflections included in the refinement: 0.0945
• Goodness-of-fit parameter for all reflections included in the refinement: 1.117
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No