Information card for entry 4310230

Structure parameters

• Formula: C44 H148 Cu7 K14 N8 O183 Si3 W33
• Calculated formula: C44 H32 Cu6.9936 K10 N8 O180 Si3 W33.0064
• Title of publication: Inorganic-Metalorganic Hybrids Based on Copper(II)-Monosubstituted Keggin Polyanions and Dinuclear Copper(II)-Oxalate Complexes. Synthesis, X-ray Structural Characterization, and Magnetic Properties
• Authors of publication: Santiago Reinoso; Pablo Vitoria; Juan M. Gutiérrez-Zorrilla; Luis Lezama; Leire San Felices; Javier I. Beitia
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Pages of publication: 9731 - 9742
• a: 12.546 ± 0.002 Å
• b: 21.303 ± 0.003 Å
• c: 37.932 ± 0.006 Å
• α: 90°
• β: 106.16 ± 0.01°
• γ: 90°
• Cell volume: 9737 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 12
• Hermann-Mauguin space group symbol: A 1 2/m 1
• Hall space group symbol: -A 2y
• Residual factor for all reflections: 0.1674
• Residual factor for significantly intense reflections: 0.0705
• Weighted residual factors for significantly intense reflections: 0.1758
• Weighted residual factors for all reflections included in the refinement: 0.1991
• Goodness-of-fit parameter for all reflections included in the refinement: 0.945
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No