Information card for entry 4310251

Structure parameters

• Formula: C50 H114 I Mo6 N3 O24
• Calculated formula: C50 H114 I Mo6 N3 O24
• Title of publication: Methoxide of an Anderson-Type Polyoxometalate and Its Conversion to a New Type of Species, [IMo9O32(OH)(OH2)3]4-
• Authors of publication: Daisuke Honda; Tomoji Ozeki; Atsushi Yagasaki
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Pages of publication: 9616 - 9618
• a: 10.4009 ± 0.0001 Å
• b: 14.6658 ± 0.0003 Å
• c: 23.5395 ± 0.0004 Å
• α: 90°
• β: 100.324 ± 0.001°
• γ: 90°
• Cell volume: 3532.52 ± 0.1 ų
• Cell temperature: 83 ± 2 K
• Ambient diffraction temperature: 85 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0393
• Residual factor for significantly intense reflections: 0.0343
• Weighted residual factors for significantly intense reflections: 0.0758
• Weighted residual factors for all reflections included in the refinement: 0.0788
• Goodness-of-fit parameter for all reflections included in the refinement: 1.196
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No