Information card for entry 4310489

Structure parameters

• Formula: C35.5 H39.25 Ag2 F12 N14.25 O2.25 P0.78 Sb1.22
• Calculated formula: C35.5 H39.25 Ag2 F12 N14.25 O2.25 P0.78 Sb1.2218
• Title of publication: Supramolecular Structural Variations with Changes in Anion and Solvent in Silver(I) Complexes of a Semirigid, Bitopic Tris(pyrazolyl)methane Ligand
• Authors of publication: Daniel L. Reger; Radu F. Semeniuc; Vitaly Rassolov; Mark D. Smith
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 537 - 554
• a: 10.4348 ± 0.0011 Å
• b: 15.3224 ± 0.0016 Å
• c: 15.8339 ± 0.0016 Å
• α: 78.255 ± 0.002°
• β: 77.464 ± 0.002°
• γ: 78.424 ± 0.002°
• Cell volume: 2386.9 ± 0.4 ų
• Cell temperature: 190 ± 2 K
• Ambient diffraction temperature: 190 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0492
• Residual factor for significantly intense reflections: 0.0389
• Weighted residual factors for significantly intense reflections: 0.0943
• Weighted residual factors for all reflections included in the refinement: 0.0972
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No