Information card for entry 4310618

Structure parameters

• Formula: C68 H104 Al2 N5 O3
• Calculated formula: C68 H104 Al2 N5 O3
• Title of publication: Synthesis and Structural Characterization of a Terminal Hydroxide Containing Alumoxane via Hydrolysis of Aluminum Hydrides
• Authors of publication: Ying Peng; Guangcai Bai; Hongjun Fan; Denis Vidovic; Herbert W. Roesky; Jörg Magull
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 1217 - 1219
• a: 14.128 ± 0.003 Å
• b: 21.5 ± 0.004 Å
• c: 22.083 ± 0.004 Å
• α: 90°
• β: 98.01 ± 0.03°
• γ: 90°
• Cell volume: 6642 ± 2 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1009
• Residual factor for significantly intense reflections: 0.0484
• Weighted residual factors for significantly intense reflections: 0.0935
• Weighted residual factors for all reflections included in the refinement: 0.1035
• Goodness-of-fit parameter for all reflections included in the refinement: 0.722
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No