Information card for entry 4310687

Structure parameters

• Formula: C44 H72 F12 N8 Ni2 O4 P2
• Calculated formula: C44 H72 F12 N8 Ni2 O4 P2
• Title of publication: Oxamidate-Bridged Dinuclear Five-Coordinate Nickel(II) Complexes: A Magneto-Structural Study
• Authors of publication: M. Dolores Santana; Gabriel García; Miguel Julve; Francesc Lloret; José Pérez; Malva Liu; Francisco Sanz; Joan Cano; Gregorio López
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 2132 - 2140
• a: 13.854 ± 0.003 Å
• b: 17.469 ± 0.004 Å
• c: 12.543 ± 0.003 Å
• α: 90°
• β: 116.22 ± 0.03°
• γ: 90°
• Cell volume: 2723.3 ± 1.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1526
• Residual factor for significantly intense reflections: 0.05
• Weighted residual factors for significantly intense reflections: 0.1039
• Weighted residual factors for all reflections included in the refinement: 0.132
• Goodness-of-fit parameter for all reflections included in the refinement: 0.852
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No