Information card for entry 4310735

Structure parameters

• Formula: C146 H114 B2 F48 O8 P4 Ru2
• Calculated formula: C146 H114 B2 F48 O8 P4 Ru2
• Title of publication: X-ray Diffraction and NMR Studies on a Series of Binap-Based Ru(II) Hydroxyphosphine π-Arene Complexes
• Authors of publication: Tilmann J. Geldbach; Frank Breher; Volker Gramlich; P. G. Anil Kumar; Paul S. Pregosin
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 1920 - 1928
• a: 14.154 ± 0.004 Å
• b: 16.131 ± 0.005 Å
• c: 16.602 ± 0.005 Å
• α: 108.787 ± 0.006°
• β: 92.473 ± 0.006°
• γ: 102.81 ± 0.006°
• Cell volume: 3472.2 ± 1.8 ų
• Cell temperature: 233 ± 2 K
• Ambient diffraction temperature: 233 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0906
• Residual factor for significantly intense reflections: 0.0494
• Weighted residual factors for significantly intense reflections: 0.121
• Weighted residual factors for all reflections included in the refinement: 0.1368
• Goodness-of-fit parameter for all reflections included in the refinement: 0.956
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No