Crystallography Open Database

Information card for entry 4310822

Preview

Coordinates	4310822.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C17 H25.5 B3 F12 Mo2 N7.5 O2
Calculated formula	C17 H25.5 B3 F12.0015 Mo2 N7.5 O2
Title of publication	Systematic Preparation of Mo24+ Building Blocks for Supramolecular Assemblies
Authors of publication	F. Albert Cotton; Chun Y. Liu; Carlos A. Murillo
Journal of publication	Inorganic Chemistry
Year of publication	2004
Journal volume	43
Pages of publication	2267 - 2276
a	11.1461 ± 0.0007 Å
b	16.2197 ± 0.0011 Å
c	19.1059 ± 0.0013 Å
α	101.377 ± 0.001°
β	95.957 ± 0.001°
γ	106.34 ± 0.001°
Cell volume	3202.5 ± 0.4 Å³
Cell temperature	213 ± 2 K
Ambient diffraction temperature	213 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0663
Residual factor for significantly intense reflections	0.0481
Weighted residual factors for significantly intense reflections	0.1166
Weighted residual factors for all reflections included in the refinement	0.1279
Goodness-of-fit parameter for all reflections included in the refinement	1.077
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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