Information card for entry 4310828

Structure parameters

• Formula: C55 H48 B Cl4 F4 N3 P4
• Calculated formula: C55 H48 B Cl4 F4 N3 P4
• Title of publication: Transformation between Diphosphinoamines and Iminobiphosphines: a Reversible PNP \λeftarrow→NP-P Rearrangement Triggered by Protonation/Deprotonation
• Authors of publication: Zhaofu Fei; Nermin Biricik; Dongbin Zhao; Rosario Scopelliti; Paul J. Dyson
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 2228 - 2230
• a: 19.359 ± 0.004 Å
• b: 19.501 ± 0.004 Å
• c: 14.1785 ± 0.0018 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5352.7 ± 1.7 ų
• Cell temperature: 140 ± 2 K
• Ambient diffraction temperature: 140 ± 2 K
• Number of distinct elements: 7
• Space group number: 52
• Hermann-Mauguin space group symbol: P n n a
• Hall space group symbol: -P 2a 2bc
• Residual factor for all reflections: 0.0738
• Residual factor for significantly intense reflections: 0.056
• Weighted residual factors for significantly intense reflections: 0.1604
• Weighted residual factors for all reflections included in the refinement: 0.1772
• Goodness-of-fit parameter for all reflections included in the refinement: 1.176
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No