Information card for entry 4310862

Structure parameters

• Formula: C38 H39 N4 Ni2 O11.7 Pb
• Calculated formula: C38 H39 N4 Ni2 O11.806 Pb
• Title of publication: Toward Rational Control of Metal Stoichiometry in Heterobimetallic Coordination Complexes: Synthesis and Characterization of Pb(Hsal)2(Cu(salen*))2, [Pb(NO3)(Cu(salen*))2](NO3), Pb(OAc)2(Cu(salen*)), and [Pb(OAc)(Ni(salen*))2](OAc)
• Authors of publication: John H. Thurston; Christopher G.-Z. Tang; Daniel W. Trahan; Kenton H. Whitmire
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 2708 - 2713
• a: 18.688 ± 0.004 Å
• b: 26.355 ± 0.005 Å
• c: 13.377 ± 0.003 Å
• α: 90°
• β: 133.01 ± 0.03°
• γ: 90°
• Cell volume: 4818 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0758
• Residual factor for significantly intense reflections: 0.0533
• Weighted residual factors for significantly intense reflections: 0.1626
• Weighted residual factors for all reflections included in the refinement: 0.1769
• Goodness-of-fit parameter for all reflections included in the refinement: 1.139
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No