Information card for entry 4310864

Structure parameters

• Formula: C36 H36 Cu2 N5 O12 Pb
• Calculated formula: C36 H36 Cu2 N5 O12 Pb
• SMILES: [Pb]12([O]3[Cu]45[O]1c1c(OC)cccc1C=[N]5CC[N]4=Cc1c3c(ccc1)OC)([O]1[Cu]34[O]2c2c(OC)cccc2C=[N]4CC[N]3=Cc2c1c(ccc2)OC)ON(=O)=O.O
• Title of publication: Toward Rational Control of Metal Stoichiometry in Heterobimetallic Coordination Complexes: Synthesis and Characterization of Pb(Hsal)2(Cu(salen*))2, [Pb(NO3)(Cu(salen*))2](NO3), Pb(OAc)2(Cu(salen*)), and [Pb(OAc)(Ni(salen*))2](OAc)
• Authors of publication: John H. Thurston; Christopher G.-Z. Tang; Daniel W. Trahan; Kenton H. Whitmire
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 2708 - 2713
• a: 22.868 ± 0.005 Å
• b: 15.543 ± 0.003 Å
• c: 23.434 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8329 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0847
• Residual factor for significantly intense reflections: 0.0582
• Weighted residual factors for significantly intense reflections: 0.2004
• Weighted residual factors for all reflections included in the refinement: 0.2278
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No