Information card for entry 4310895

Structure parameters

• Formula: C16 H41 Cl2 N8 O16.5 Pb
• Calculated formula: C16 H41 Cl2 N8 O16.5 Pb
• Title of publication: Structural Effects of the Lone Pair on Lead(II), and Parallels with the Coordination Geometry of Mercury(II). Does the Lone Pair on Lead(II) Form H-Bonds? Structures of the Lead(II) and Mercury(II) Complexes of the Pendant-Donor Macrocycle DOTAM (1,4,7,10-Tetrakis(carbamoylmethyl)-1,4,7,10-tetraazacyclododecane)
• Authors of publication: Robert D. Hancock; Joseph H. Reibenspies; Hulisani Maumela
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 2981 - 2987
• a: 12.767 ± 0.003 Å
• b: 13.528 ± 0.004 Å
• c: 18.385 ± 0.005 Å
• α: 101.45 ± 0.02°
• β: 93.32 ± 0.02°
• γ: 90.53 ± 0.02°
• Cell volume: 3106.2 ± 1.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0904
• Residual factor for significantly intense reflections: 0.05
• Weighted residual factors for all reflections: 0.124
• Weighted residual factors for significantly intense reflections: 0.0984
• Goodness-of-fit parameter for all reflections: 1.097
• Goodness-of-fit parameter for significantly intense reflections: 1.092
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKa
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No