Information card for entry 4310901

Structure parameters

• Formula: C12 H41 N6 O24.5 V2
• Calculated formula: C12 H40 N6 O24.5 V2
• Title of publication: pH-Specific Synthesis of a Dinuclear Vanadium(V)-Peroxo-Citrate Complex in Aqueous Solutions: pH-Dependent Linkage, Spectroscopic and Structural Correlations with Other Aqueous Vanadium(V)-Peroxo-Citrate and Non-Peroxo Species
• Authors of publication: M. Kaliva; C. P. Raptopoulou; A. Terzis; A. Salifoglou
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 2895 - 2905
• a: 12.391 ± 0.005 Å
• b: 15.737 ± 0.007 Å
• c: 17.102 ± 0.007 Å
• α: 90°
• β: 110.84 ± 0.01°
• γ: 90°
• Cell volume: 3117 ± 2 ų
• Cell temperature: 298 K
• Ambient diffraction temperature: 298 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0644
• Residual factor for significantly intense reflections: 0.0519
• Weighted residual factors for all reflections: 0.1623
• Weighted residual factors for significantly intense reflections: 0.1475
• Goodness-of-fit parameter for all reflections: 1.051
• Goodness-of-fit parameter for significantly intense reflections: 1.074
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No