Information card for entry 4310921

Structure parameters

• Formula: Ge16 Na9.592 O40
• Calculated formula: Ge16 Na9.592 O40
• Title of publication: Synthesis, Structural Characterization, and Thermal Stability of a New Layered Germanate Structure, Na4Ge16O28(OH)12
• Authors of publication: Annemieke W. C. van den Berg; Govert Baak; Hendrikus van Koningsveld; Jacobus C. Jansen; Thomas Maschmeyer
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 2888 - 2894
• a: 7.3216 ± 0.0006 Å
• b: 14.3986 ± 0.0009 Å
• c: 7.7437 ± 0.0006 Å
• α: 90°
• β: 100.179 ± 0.007°
• γ: 90°
• Cell volume: 803.5 ± 0.11 ų
• Cell temperature: 293 K
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 3
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.09
• Residual factor for significantly intense reflections: 0.069
• Weighted residual factors for all reflections: 0.078
• Weighted residual factors for all reflections included in the refinement: 0.078
• Goodness-of-fit parameter for all reflections: 5.151
• Goodness-of-fit parameter for all reflections included in the refinement: 5.689
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No