Information card for entry 4311050

Structure parameters

• Formula: C30 H76 Li2 N8 P2 Si2
• Calculated formula: C30 H76 Li2 N8 P2 Si2
• Title of publication: Lithiation of (tBuNH)3PNSiMe3 and Formation of Tetraimidophosphate Complexes Containing M3O3 Rings (M = Li, K): X-ray Structure of the Stable Radical {(Me3SiN)P(μ3-NtBu)3[μ3-Li(THF)]3(OtBu)}
• Authors of publication: Andrea Armstrong; Tristram Chivers; Masood Parvez; Gabriele Schatte; René T. Boeré
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 3453 - 3460
• a: 13.4399 ± 0.0003 Å
• b: 15.7195 ± 0.0005 Å
• c: 20.3644 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4302.4 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0774
• Residual factor for significantly intense reflections: 0.0506
• Weighted residual factors for significantly intense reflections: 0.1148
• Weighted residual factors for all reflections included in the refinement: 0.1293
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No