Information card for entry 4311353

Structure parameters

• Formula: C21 H14 Cl2 N3 O9 Rh3
• Calculated formula: C21 H14 Cl2 N3 O9 Rh3
• SMILES: [Rh]123([Rh]4([Cl][Rh](Cl)(C#[O])C#[O])([O]=C(OC)c5c([N]4=NN3c3c(C(=[O]2)OC)cccc3)cccc5)(C1=O)C#[O])C#[O]
• Title of publication: Crescent-Shaped Rhodium(I) Complexes with Bis(o-carboxymethylphenyl)triazenide
• Authors of publication: Cristina Tejel; Miguel A. Ciriano; Gustavo Ríos-Moreno; Isabel T. Dobrinovitch; Fernando J. Lahoz; Luis A. Oro; Miguel Parra-Hake
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 4719 - 4726
• a: 9.576 ± 0.0006 Å
• b: 9.7734 ± 0.0006 Å
• c: 14.6622 ± 0.0009 Å
• α: 94.942 ± 0.001°
• β: 92.982 ± 0.001°
• γ: 108.777 ± 0.001°
• Cell volume: 1289.74 ± 0.14 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0383
• Residual factor for significantly intense reflections: 0.0303
• Weighted residual factors for significantly intense reflections: 0.0548
• Weighted residual factors for all reflections included in the refinement: 0.0561
• Goodness-of-fit parameter for all reflections included in the refinement: 0.973
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No