Information card for entry 4311515

Structure parameters

• Formula: C50.75 H50 Cl2 O8.25 P4 U
• Calculated formula: C50.75 H47 Cl2 O8.25 P4 U
• Title of publication: Spectroscopic Evidence for the Direct Coordination of the Pertechnetate Anion to the Uranyl Cation in [UO2(TcO4)(DPPMO2)2]+
• Authors of publication: Andrew D. Sutton; Gordon H. John; Mark J. Sarsfield; Joanna C. Renshaw; Iain May; Leigh R. Martin; Andrew J. Selvage; David Collison; Madeleine Helliwell
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 5480 - 5482
• a: 14.5893 ± 0.0016 Å
• b: 19.282 ± 0.002 Å
• c: 19.991 ± 0.002 Å
• α: 73.868 ± 0.002°
• β: 87.715 ± 0.002°
• γ: 81.923 ± 0.002°
• Cell volume: 5348.7 ± 1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0721
• Residual factor for significantly intense reflections: 0.0518
• Weighted residual factors for significantly intense reflections: 0.125
• Weighted residual factors for all reflections included in the refinement: 0.1356
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No