Information card for entry 4311830

Structure parameters

• Formula: C100 H106 Fe4 N24 Ni4 O21
• Calculated formula: C100 H72 Fe4 N24 Ni4 O20.95
• Title of publication: Octanuclear Metallocyclic Ni4Fc4 Compound: Synthesis, Crystal Structure, and Electrochemical Sensing for Mg2+
• Authors of publication: Mingxue Li; Ping Cai; Chunying Duan; Feng Lu; Jin Xie; Qingjin Meng
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 5174 - 5176
• a: 18.367 ± 0.002 Å
• b: 24.646 ± 0.003 Å
• c: 25.691 ± 0.003 Å
• α: 90°
• β: 92.973 ± 0.003°
• γ: 90°
• Cell volume: 11614 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.3289
• Residual factor for significantly intense reflections: 0.0767
• Weighted residual factors for significantly intense reflections: 0.1142
• Weighted residual factors for all reflections included in the refinement: 0.1517
• Goodness-of-fit parameter for all reflections included in the refinement: 0.837
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No