Information card for entry 4311832

Structure parameters

• Chemical name: bis-(2,2':6',2'':6'',2'''-quaterpyridine)-nickel diperchlorate tetrahydrate
• Formula: C40 H36 Cl2 N8 Ni O12
• Calculated formula: C40 H28 Cl2 N8 Ni O12
• Title of publication: Bis-qtpy (qtpy = 2,2':6',2'':6'',2'''-quaterpyridine) Metal Complexes, [M(qtpy)~2~]^2+^
• Authors of publication: Belli Dell'Amico, Daniela; Fausto Calderazzo; Matteo Curiardi; Luca Labella; Fabio Marchetti
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 5459 - 5465
• a: 24.353 ± 0.008 Å
• b: 8.1 ± 0.0016 Å
• c: 22.624 ± 0.006 Å
• α: 90°
• β: 108.49 ± 0.03°
• γ: 90°
• Cell volume: 4232 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0931
• Residual factor for significantly intense reflections: 0.0912
• Weighted residual factors for significantly intense reflections: 0.2699
• Weighted residual factors for all reflections included in the refinement: 0.2784
• Goodness-of-fit parameter for all reflections included in the refinement: 1.429
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No