Information card for entry 4312178

Structure parameters

• Formula: C10 H52 As8 Cl N10 Ni3.5 O47 V13
• Calculated formula: C10 H34 As8 Cl N10 Ni3.5 O47 V13
• Title of publication: A Novel Chainlike As-V-O Polymer Based on a Transition Metal Complex and a Dimeric Polyoxoanion
• Authors of publication: Xiao-Bing Cui; Ji-Qing Xu; He Meng; Shou-Tian Zheng; Guo-Yu Yang
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 8005 - 8009
• a: 13.358 ± 0.003 Å
• b: 14.198 ± 0.003 Å
• c: 19.723 ± 0.004 Å
• α: 83.88 ± 0.03°
• β: 86.04 ± 0.03°
• γ: 64.66 ± 0.03°
• Cell volume: 3360.3 ± 1.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0697
• Residual factor for significantly intense reflections: 0.0536
• Weighted residual factors for significantly intense reflections: 0.1435
• Weighted residual factors for all reflections included in the refinement: 0.1569
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No