Information card for entry 4312198

Structure parameters

• Formula: C8 H20 N O3 Re S
• Calculated formula: C8 H20 N O3 Re S
• Title of publication: Oxygen/Sulfur Substitution Reactions of Tetraoxometalates Effected by Electrophilic Carbon and Silicon Reagents
• Authors of publication: David V. Partyka; R. H. Holm
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 8609 - 8616
• a: 7.133 ± 0.0014 Å
• b: 21.366 ± 0.004 Å
• c: 16.628 ± 0.003 Å
• α: 90°
• β: 91.38 ± 0.03°
• γ: 90°
• Cell volume: 2533.4 ± 0.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1103
• Residual factor for significantly intense reflections: 0.0968
• Weighted residual factors for significantly intense reflections: 0.1864
• Weighted residual factors for all reflections included in the refinement: 0.1911
• Goodness-of-fit parameter for all reflections included in the refinement: 1.276
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No