Information card for entry 4312210

Structure parameters

• Formula: C75 H78 B2 Cl6 F8 P4 Rh2 S4
• Calculated formula: C75 H78 B2 Cl6 F8 P4 Rh2 S4
• Title of publication: Heteroligated Metallomacrocycles Generated via the Weak-Link Approach
• Authors of publication: Maxim V. Ovchinnikov; Aaron M. Brown; Xiaogang Liu; Chad A. Mirkin; Lev N. Zakharov; Arnold L. Rheingold
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 8233 - 8235
• a: 10.5464 ± 0.0007 Å
• b: 14.9351 ± 0.0009 Å
• c: 25.1498 ± 0.0016 Å
• α: 86.123 ± 0.001°
• β: 78.705 ± 0.001°
• γ: 86.78 ± 0.001°
• Cell volume: 3872 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0599
• Residual factor for significantly intense reflections: 0.0454
• Weighted residual factors for significantly intense reflections: 0.1052
• Weighted residual factors for all reflections included in the refinement: 0.1129
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No