Information card for entry 4312401

Structure parameters

• Formula: C38 H42 Cl3 F6 N2 P3 Rh2
• Calculated formula: C38 H44 Cl3 F6 N2 P3 Rh2
• Title of publication: Diphosphines Possessing Electronically Different Donor Groups: Synthesis and Coordination Chemistry of the Unsymmetrical Di(N-pyrrolyl)phosphino-Functionalized dppm Analogue Ph2PCH2P(NC4H4)2
• Authors of publication: Andrew D. Burrows; Mary F. Mahon; Steven P. Nolan; Maurizio Varrone
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 7227 - 7238
• a: 15.615 ± 0.0004 Å
• b: 16.64 ± 0.0004 Å
• c: 15.791 ± 0.0004 Å
• α: 90°
• β: 92.146 ± 0.001°
• γ: 90°
• Cell volume: 4100.15 ± 0.18 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0743
• Residual factor for significantly intense reflections: 0.0407
• Weighted residual factors for significantly intense reflections: 0.0938
• Weighted residual factors for all reflections included in the refinement: 0.1099
• Goodness-of-fit parameter for all reflections included in the refinement: 0.978
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No