Crystallography Open Database

Information card for entry 4312468

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Coordinates	4312468.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C38 H45 Cl Li O3 Sm
Calculated formula	C32 H32.128 Cl Li O3 Sm
Title of publication	Terphenyl Cyclooctatetraenyl Compounds of Samarium
Authors of publication	Gerd W. Rabe; Mei Zhang-Presse; Florian A. Riederer; James A. Golen; Christopher D. Incarvito; Arnold L. Rheingold
Journal of publication	Inorganic Chemistry
Year of publication	2003
Journal volume	42
Pages of publication	7587 - 7592
a	12.7753 ± 0.0008 Å
b	16.8698 ± 0.001 Å
c	16.9344 ± 0.0011 Å
α	90°
β	103.495 ± 0.001°
γ	90°
Cell volume	3548.9 ± 0.4 Å³
Cell temperature	147 ± 2 K
Ambient diffraction temperature	147 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0431
Residual factor for significantly intense reflections	0.0344
Weighted residual factors for significantly intense reflections	0.0819
Weighted residual factors for all reflections included in the refinement	0.0872
Goodness-of-fit parameter for all reflections included in the refinement	1.042
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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