Information card for entry 4312549

Structure parameters

• Formula: C49 H34 B2 Cl2 F8 O8 P4 Pd
• Calculated formula: C49 H34 B2 Cl2 F8 O8 P4 Pd
• Title of publication: Enolphosphato-Phosphines: A New Class of P,O Ligands
• Authors of publication: Xavier Morise; Pierre Braunstein; Richard Welter
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 7752 - 7765
• a: 17.133 Å
• b: 22.051 Å
• c: 14.681 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5546.48 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 52
• Hermann-Mauguin space group symbol: P n n a
• Hall space group symbol: -P 2a 2bc
• Residual factor for all reflections: 0.0764
• Residual factor for significantly intense reflections: 0.0582
• Weighted residual factors for significantly intense reflections: 0.1615
• Weighted residual factors for all reflections included in the refinement: 0.1845
• Goodness-of-fit parameter for all reflections included in the refinement: 0.921
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No