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Information card for entry 4313097
Preview
Coordinates | 4313097.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C83 H148 N4 O16 Si8 Zn4 |
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Calculated formula | C83 H148 N4 O16 Si8 Zn4 |
SMILES | [Si@]1(O)(N([Si](C)(C)C)c2c(cccc2C(C)C)C(C)C)O[Zn]2([O]3CCCC3)[O]3[Zn]4([O]2[Si@](N([Si](C)(C)C)c2c(cccc2C(C)C)C(C)C)(O)O[Zn]2([O]1[Zn](O[Si@@]3(N([Si](C)(C)C)c1c(cccc1C(C)C)C(C)C)O)([O]2[Si@@](N([Si](C)(C)C)c1c(cccc1C(C)C)C(C)C)(O)O4)[O]1CCCC1)[O]1CCCC1)[O]1CCCC1.c1(ccccc1)C |
Title of publication | Synthesis and X-ray Crystal Structure of [(THF)Zn(O2(OH)SiR)]4 (R = (2,6-i-Pr2C6H3)N(SiMe3)): Enroute to Larger Aggregates |
Authors of publication | Ganapathi Anantharaman; Herbert W. Roesky; Hans-Georg Schmidt; Mathias Noltemeyer; Jiri Pinkas |
Journal of publication | Inorganic Chemistry |
Year of publication | 2003 |
Journal volume | 42 |
Pages of publication | 970 - 973 |
a | 17.117 ± 0.003 Å |
b | 16.692 ± 0.005 Å |
c | 17.399 ± 0.004 Å |
α | 90° |
β | 91.45 ± 0.07° |
γ | 90° |
Cell volume | 4970 ± 2 Å3 |
Cell temperature | 200 ± 2 K |
Ambient diffraction temperature | 200 ± 2 K |
Number of distinct elements | 6 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0775 |
Residual factor for significantly intense reflections | 0.0569 |
Weighted residual factors for significantly intense reflections | 0.1386 |
Weighted residual factors for all reflections included in the refinement | 0.1536 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.05 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4313097.html
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