Information card for entry 4313097

Structure parameters

• Formula: C83 H148 N4 O16 Si8 Zn4
• Calculated formula: C83 H148 N4 O16 Si8 Zn4
• SMILES: [Si@]1(O)(N([Si](C)(C)C)c2c(cccc2C(C)C)C(C)C)O[Zn]2([O]3CCCC3)[O]3[Zn]4([O]2[Si@](N([Si](C)(C)C)c2c(cccc2C(C)C)C(C)C)(O)O[Zn]2([O]1[Zn](O[Si@@]3(N([Si](C)(C)C)c1c(cccc1C(C)C)C(C)C)O)([O]2[Si@@](N([Si](C)(C)C)c1c(cccc1C(C)C)C(C)C)(O)O4)[O]1CCCC1)[O]1CCCC1)[O]1CCCC1.c1(ccccc1)C
• Title of publication: Synthesis and X-ray Crystal Structure of [(THF)Zn(O2(OH)SiR)]4 (R = (2,6-i-Pr2C6H3)N(SiMe3)): Enroute to Larger Aggregates
• Authors of publication: Ganapathi Anantharaman; Herbert W. Roesky; Hans-Georg Schmidt; Mathias Noltemeyer; Jiri Pinkas
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 970 - 973
• a: 17.117 ± 0.003 Å
• b: 16.692 ± 0.005 Å
• c: 17.399 ± 0.004 Å
• α: 90°
• β: 91.45 ± 0.07°
• γ: 90°
• Cell volume: 4970 ± 2 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0775
• Residual factor for significantly intense reflections: 0.0569
• Weighted residual factors for significantly intense reflections: 0.1386
• Weighted residual factors for all reflections included in the refinement: 0.1536
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No