Information card for entry 4313099

Structure parameters

• Formula: C54 H58 Cl8 Co2 N12 O4
• Calculated formula: C54 H58 Cl8 Co2 N12 O4
• Title of publication: Dinuclear Cyano Complexes of Cobalt(III) and Iron(III) Containing Noninnocent 1,2,4,5-Tetrakis(2-pyridinecarboxamido)benzene Bridging Ligands
• Authors of publication: Udo Beckmann; Eckhard Bill; Thomas Weyhermüller; Karl Wieghardt
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 1045 - 1056
• a: 10.3351 ± 0.0008 Å
• b: 13.1244 ± 0.001 Å
• c: 13.3233 ± 0.0011 Å
• α: 113.72 ± 0.02°
• β: 103.35 ± 0.02°
• γ: 102.22 ± 0.02°
• Cell volume: 1512.8 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0991
• Residual factor for significantly intense reflections: 0.0519
• Weighted residual factors for all reflections: 0.1222
• Weighted residual factors for significantly intense reflections: 0.1092
• Goodness-of-fit parameter for all reflections: 0.909
• Goodness-of-fit parameter for significantly intense reflections: 1.044
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No