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Information card for entry 4313118
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Coordinates | 4313118.cif |
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Original paper (by DOI) | HTML |
Formula | C28 H63 B O9 Si2 |
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Calculated formula | C28 H63 B O9 Si2 |
Title of publication | Tris(tert-butoxy)siloxy Derivatives of Boron, Including the Boronous Acid HOB[OSi(OtBu)3]2 and the Metal (Siloxy)boryloxide Complex Cp2Zr(Me)OB[OSi(OtBu)3]2: A Remarkable Crystal Structure with 18 Independent Molecules in Its Asymmetric Unit |
Authors of publication | Kyle L. Fujdala; Allen G. Oliver; Frederick J. Hollander; T. Don Tilley |
Journal of publication | Inorganic Chemistry |
Year of publication | 2003 |
Journal volume | 42 |
Pages of publication | 1140 - 1150 |
a | 9.4639 ± 0.0005 Å |
b | 11.8965 ± 0.0004 Å |
c | 17.8225 ± 0.0011 Å |
α | 93.089 ± 0.003° |
β | 101.872 ± 0.001° |
γ | 101.34 ± 0.003° |
Cell volume | 1916 ± 0.17 Å3 |
Cell temperature | 159 ± 2 K |
Ambient diffraction temperature | 159 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1356 |
Residual factor for significantly intense reflections | 0.0825 |
Weighted residual factors for all reflections | 0.2475 |
Weighted residual factors for significantly intense reflections | 0.2116 |
Goodness-of-fit parameter for all reflections | 0.983 |
Goodness-of-fit parameter for significantly intense reflections | 1.127 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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