Information card for entry 4313118

Structure parameters

• Formula: C28 H63 B O9 Si2
• Calculated formula: C28 H63 B O9 Si2
• Title of publication: Tris(tert-butoxy)siloxy Derivatives of Boron, Including the Boronous Acid HOB[OSi(OtBu)3]2 and the Metal (Siloxy)boryloxide Complex Cp2Zr(Me)OB[OSi(OtBu)3]2: A Remarkable Crystal Structure with 18 Independent Molecules in Its Asymmetric Unit
• Authors of publication: Kyle L. Fujdala; Allen G. Oliver; Frederick J. Hollander; T. Don Tilley
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 1140 - 1150
• a: 9.4639 ± 0.0005 Å
• b: 11.8965 ± 0.0004 Å
• c: 17.8225 ± 0.0011 Å
• α: 93.089 ± 0.003°
• β: 101.872 ± 0.001°
• γ: 101.34 ± 0.003°
• Cell volume: 1916 ± 0.17 ų
• Cell temperature: 159 ± 2 K
• Ambient diffraction temperature: 159 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1356
• Residual factor for significantly intense reflections: 0.0825
• Weighted residual factors for all reflections: 0.2475
• Weighted residual factors for significantly intense reflections: 0.2116
• Goodness-of-fit parameter for all reflections: 0.983
• Goodness-of-fit parameter for significantly intense reflections: 1.127
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No