Information card for entry 4313146

Structure parameters

• Common name: [Li(DME)3]2[Fe2(mu-NPh)2Cl4]
• Formula: C36 H70 Cl4 Fe2 Li2 N2 O12
• Calculated formula: C36 H70 Cl4 Fe2 Li2 N2 O12
• Title of publication: Iron-Arylimide Clusters [Fem(NAr)nCl4]2- (m,n= 2, 2; 3, 4; 4, 4) from a Ferric Amide Precursor: Synthesis, Characterization, and Comparison to Fe-S Chemistry
• Authors of publication: Jeremiah S. Duncan; Tamim M. Nazif; Atul K. Verma; Sonny C. Lee
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 1211 - 1224
• a: 29.2305 ± 0.0014 Å
• b: 11.6925 ± 0.0005 Å
• c: 19.0941 ± 0.0008 Å
• α: 90°
• β: 128.378 ± 0.002°
• γ: 90°
• Cell volume: 5115.9 ± 0.4 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0708
• Residual factor for significantly intense reflections: 0.0437
• Weighted residual factors for all reflections: 0.124
• Weighted residual factors for significantly intense reflections: 0.1078
• Goodness-of-fit parameter for all reflections: 1.015
• Goodness-of-fit parameter for significantly intense reflections: 1.051
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No