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Information card for entry 4313148
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Coordinates | 4313148.cif |
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Original paper (by DOI) | HTML |
Common name | [Li(DME)3]2[Fe4(mu3-NPh)4Cl4].DME |
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Formula | C52 H90 Cl4 Fe4 Li2 N4 O14 |
Calculated formula | C52 H90 Cl4 Fe4 Li2 N4 O14 |
Title of publication | Iron-Arylimide Clusters [Fem(NAr)nCl4]2- (m,n= 2, 2; 3, 4; 4, 4) from a Ferric Amide Precursor: Synthesis, Characterization, and Comparison to Fe-S Chemistry |
Authors of publication | Jeremiah S. Duncan; Tamim M. Nazif; Atul K. Verma; Sonny C. Lee |
Journal of publication | Inorganic Chemistry |
Year of publication | 2003 |
Journal volume | 42 |
Pages of publication | 1211 - 1224 |
a | 12.5052 ± 0.0006 Å |
b | 15.2469 ± 0.0008 Å |
c | 35.828 ± 0.002 Å |
α | 90° |
β | 96.323 ± 0.002° |
γ | 90° |
Cell volume | 6789.6 ± 0.6 Å3 |
Cell temperature | 200 ± 2 K |
Ambient diffraction temperature | 200 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0993 |
Residual factor for significantly intense reflections | 0.0511 |
Weighted residual factors for all reflections | 0.1486 |
Weighted residual factors for significantly intense reflections | 0.1197 |
Goodness-of-fit parameter for all reflections | 1.014 |
Goodness-of-fit parameter for significantly intense reflections | 1.063 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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