Information card for entry 4313160

Structure parameters

• Formula: C70 H72 Li N5 O4 P4 Pd2
• Calculated formula: C83 H72 Li N5 O4 P4 Pd2
• Title of publication: Platinum and Palladium Imido and Oxo Complexes with Small Natural Bite Angle Diphosphine Ligands
• Authors of publication: U. Anandhi; Todd Holbert; Dennis Lueng; Paul R. Sharp
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 1282 - 1295
• a: 11.5079 ± 0.001 Å
• b: 24.026 ± 0.002 Å
• c: 13.7686 ± 0.0012 Å
• α: 90°
• β: 100.951 ± 0.002°
• γ: 90°
• Cell volume: 3737.5 ± 0.6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.1562
• Residual factor for significantly intense reflections: 0.087
• Weighted residual factors for significantly intense reflections: 0.1556
• Weighted residual factors for all reflections included in the refinement: 0.1793
• Goodness-of-fit parameter for all reflections included in the refinement: 1.094
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No