Information card for entry 4313164

Structure parameters

• Formula: C55 H57 F6 N3 O6 P2 Pd S2
• Calculated formula: C55 H57 F6 N3 O6 P2 Pd S2
• Title of publication: Platinum and Palladium Imido and Oxo Complexes with Small Natural Bite Angle Diphosphine Ligands
• Authors of publication: U. Anandhi; Todd Holbert; Dennis Lueng; Paul R. Sharp
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 1282 - 1295
• a: 11.2832 ± 0.0011 Å
• b: 12.4429 ± 0.0012 Å
• c: 20.1851 ± 0.0019 Å
• α: 90°
• β: 100.305 ± 0.002°
• γ: 90°
• Cell volume: 2788.2 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/n 1
• Hall space group symbol: -P 2yac
• Residual factor for all reflections: 0.0952
• Residual factor for significantly intense reflections: 0.0556
• Weighted residual factors for significantly intense reflections: 0.1327
• Weighted residual factors for all reflections included in the refinement: 0.1503
• Goodness-of-fit parameter for all reflections included in the refinement: 0.91
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No