Information card for entry 4313167

Structure parameters

• Formula: C90 H116 Li N3 O4 P4 Pd2 Si2
• Calculated formula: C90 H116 Li N3 O4 P4 Pd2 Si2
• Title of publication: Platinum and Palladium Imido and Oxo Complexes with Small Natural Bite Angle Diphosphine Ligands
• Authors of publication: U. Anandhi; Todd Holbert; Dennis Lueng; Paul R. Sharp
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 1282 - 1295
• a: 13.146 ± 0.006 Å
• b: 14.948 ± 0.007 Å
• c: 24.173 ± 0.012 Å
• α: 89.291 ± 0.008°
• β: 85.35 ± 0.008°
• γ: 67.986 ± 0.008°
• Cell volume: 4388 ± 4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1351
• Residual factor for significantly intense reflections: 0.0766
• Weighted residual factors for significantly intense reflections: 0.1739
• Weighted residual factors for all reflections included in the refinement: 0.2167
• Goodness-of-fit parameter for all reflections included in the refinement: 1.068
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No