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Information card for entry 4313188
Preview
Coordinates | 4313188.cif |
---|---|
Original paper (by DOI) | HTML |
External links | ChemSpider |
Formula | C30 H33 N O2 P2 |
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Calculated formula | C30 H33 N O2 P2 |
SMILES | P(=O)(c1ccccc1)(c1ccccc1)CN(CP(=O)(c1ccccc1)c1ccccc1)CCCC |
Title of publication | Insertion of Carbon Fragments into P(III)-N Bonds in Aminophosphines and Aminobis(phosphines): Synthesis, Reactivity, and Coordination Chemistry of Resulting Phosphine Oxide Derivatives. Crystal and Molecular Structures of (Ph2P(O)CH2)2NR (R = Me,nPr,nBu), Ph2P(O)CH(OH)nPr, and cis-[MoO2Cl2{(Ph2P(O)CH2)2NEt-κO,κO}] |
Authors of publication | Srinivasan Priya; Maravanji S. Balakrishna; Joel T. Mague; Shaikh M. Mobin |
Journal of publication | Inorganic Chemistry |
Year of publication | 2003 |
Journal volume | 42 |
Pages of publication | 1272 - 1281 |
a | 8.053 ± 0.0016 Å |
b | 10.287 ± 0.002 Å |
c | 16.264 ± 0.003 Å |
α | 85.72 ± 0.03° |
β | 89.53 ± 0.03° |
γ | 89.81 ± 0.03° |
Cell volume | 1343.5 ± 0.5 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0526 |
Residual factor for significantly intense reflections | 0.0395 |
Weighted residual factors for significantly intense reflections | 0.1045 |
Weighted residual factors for all reflections included in the refinement | 0.1122 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.09 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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