Information card for entry 4313190

Structure parameters

• Formula: C28.3 H29.6 Cl2.6 Mo N O4 P2
• Calculated formula: C28.3 H29.6 Cl2.6 Mo N O4 P2
• Title of publication: Insertion of Carbon Fragments into P(III)-N Bonds in Aminophosphines and Aminobis(phosphines): Synthesis, Reactivity, and Coordination Chemistry of Resulting Phosphine Oxide Derivatives. Crystal and Molecular Structures of (Ph2P(O)CH2)2NR (R = Me,nPr,nBu), Ph2P(O)CH(OH)nPr, and cis-[MoO2Cl2{(Ph2P(O)CH2)2NEt-κO,κO}]
• Authors of publication: Srinivasan Priya; Maravanji S. Balakrishna; Joel T. Mague; Shaikh M. Mobin
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 1272 - 1281
• a: 16.822 ± 0.008 Å
• b: 16.191 ± 0.011 Å
• c: 23.722 ± 0.013 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6461 ± 6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.1487
• Residual factor for significantly intense reflections: 0.0687
• Weighted residual factors for significantly intense reflections: 0.2029
• Weighted residual factors for all reflections included in the refinement: 0.2378
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No