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Information card for entry 4313441
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Coordinates | 4313441.cif |
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Original paper (by DOI) | HTML |
Common name | Cu3(dpa)4Cl2SbCl6 2.44(acetone) |
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Formula | C47.31 H46.63 Cl8 Cu3 N12 O2.44 Sb |
Calculated formula | C47.32 H46.64 Cl8 Cu3 N12 O2.44 Sb |
Title of publication | Oxidation of Ni3(dpa)4Cl2 and Cu3(dpa)4Cl2: Nickel-Nickel Bonding Interaction, but No Copper-Copper Bonds |
Authors of publication | John F. Berry; F. Albert Cotton; Lee M. Daniels; Carlos A. Murillo; Xiaoping Wang |
Journal of publication | Inorganic Chemistry |
Year of publication | 2003 |
Journal volume | 42 |
Pages of publication | 2418 - 2427 |
a | 15.0331 ± 0.0012 Å |
b | 12.401 ± 0.001 Å |
c | 33.114 ± 0.003 Å |
α | 90° |
β | 99.506 ± 0.003° |
γ | 90° |
Cell volume | 6088.5 ± 0.9 Å3 |
Cell temperature | 173 K |
Ambient diffraction temperature | 173 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.1457 |
Residual factor for significantly intense reflections | 0.1087 |
Weighted residual factors for significantly intense reflections | 0.2152 |
Weighted residual factors for all reflections included in the refinement | 0.2416 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.167 |
Method of determination | single crystal |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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