Information card for entry 4313507

Structure parameters

• Formula: C32 H32 Cl4 N4 O Pb2 S
• Calculated formula: C32 H32 Cl4 N4 O Pb2 S
• Title of publication: Compositional and Structural Variety of Diphenyllead(IV) Complexes Obtained by Reaction of Diphenyllead Dichloride with Thiosemicarbazones
• Authors of publication: José S. Casas; Eduardo E. Castellano; J. Ellena; María S. García Tasende; Agustín Sánchez; José Sordo; María J. Vidarte
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 2584 - 2595
• a: 9.907 ± 0.002 Å
• b: 12.604 ± 0.003 Å
• c: 15.834 ± 0.004 Å
• α: 109.016 ± 0.004°
• β: 92.413 ± 0.004°
• γ: 103.377 ± 0.004°
• Cell volume: 1803.6 ± 0.7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0452
• Residual factor for significantly intense reflections: 0.0252
• Weighted residual factors for significantly intense reflections: 0.0528
• Weighted residual factors for all reflections included in the refinement: 0.0602
• Goodness-of-fit parameter for all reflections included in the refinement: 1.061
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No