Information card for entry 4313595

Structure parameters

• Formula: C166 H212 Cl8 N8 O18 Pd4
• Calculated formula: C166 H212 Cl8 N8 O18 Pd4
• Title of publication: A New Ligand System Based on a Bipyridine-Functionalized Calix[4]arene Backbone Leading to Mono- and Bimetallic Complexes
• Authors of publication: Reto Dorta; Linda J. W. Shimon; Haim Rozenberg; Yehoshoa Ben-David; David Milstein
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 3160 - 3167
• a: 11.805 ± 0.003 Å
• b: 26.644 ± 0.005 Å
• c: 28.186 ± 0.009 Å
• α: 65.82 ± 0.01°
• β: 84.54 ± 0.01°
• γ: 85.42 ± 0.01°
• Cell volume: 8043 ± 4 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0635
• Residual factor for significantly intense reflections: 0.0488
• Weighted residual factors for significantly intense reflections: 0.1083
• Weighted residual factors for all reflections included in the refinement: 0.1166
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No