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Information card for entry 4313707
Preview
Coordinates | 4313707.cif |
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Original paper (by DOI) | HTML |
Formula | C39 H28 Cl4 F10 N4 O3 Pd2 |
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Calculated formula | C39 H28 Cl4 F10 N4 O3 Pd2 |
Title of publication | Insertion Reactions into Pd-O and Pd-N Bonds: Preparation of Alkoxycarbonyl, Carbonato, Carbamato, Thiocarbamate, and Thioureide Complexes of Palladium(II) |
Authors of publication | José Ruiz; M. Teresa Martínez; Félix Florenciano; Venancio Rodríguez; Gregorio López; José Pérez; Penny A. Chaloner; Peter B. Hitchcock |
Journal of publication | Inorganic Chemistry |
Year of publication | 2003 |
Journal volume | 42 |
Pages of publication | 3650 - 3661 |
a | 11.1311 ± 0.0006 Å |
b | 11.6741 ± 0.0007 Å |
c | 17.0116 ± 0.0008 Å |
α | 70.81 ± 0.004° |
β | 84.557 ± 0.004° |
γ | 84.114 ± 0.004° |
Cell volume | 2072.3 ± 0.2 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0427 |
Residual factor for significantly intense reflections | 0.0323 |
Weighted residual factors for significantly intense reflections | 0.0829 |
Weighted residual factors for all reflections included in the refinement | 0.0873 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.869 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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